An article Visible light mediated synthesis of 4-aryl-1,2-dihydronaphthalene derivatives via single-electron oxidation or MHAT from methylenecyclopropanes WOS:000605450500012 published article about PHOTOREDOX CATALYSIS; ALKYLIDENECYCLOPROPANES; CYCLOADDITIONS; ALKYNYLIDENECYCLOPROPANES; TRANSMETALATION; HETEROCYCLES; ALKENES in [Liu, Jiaxin; Wei, Yin; Shi, Min] Chinese Acad Sci, Shanghai Inst Organ Chem, Univ Chinese Acad Sci, Ctr Excellence Mol Synth,State Key Lab Organometa, 345 Lingling Rd, Shanghai 200032, Peoples R China; [Shi, Min] Southern Univ Sci & Technol, Shenzhen Grubbs Inst, Shenzhen 518000, Guangdong, Peoples R China in 2021, Cited 76. The Name is 3-Methylbenzoic acid. Through research, I have a further understanding and discovery of 99-04-7. Recommanded Product: 3-Methylbenzoic acid
We report a direct single-electron oxidation of methylenecyclopropanes (MCPs) for the rapid construction of 4-aryl-1,2-dihydronaphthalene derivatives by merging visible light photoredox catalysis and cobalt catalysis. In MeCN with Et3N center dot 3HF (1.0 equiv.), the fluorination of MCPs can be realized in the presence of 9-mesityl-10-methylacridinium perchlorate and Co(dmgH)(2)PyCl, affording fluorinated 4-aryl-1,2-dihy-dronaphthalene derivatives in moderate yields. In MeCN/HFIP (7 : 3), 4-aryl-1,2-dihydronaphthalene derivatives were obtained in good yields through a MHAT process under similar conditions.
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