Formula: C8H8O2. Lecomte, M; Lipshultz, JM; Kim-Lee, SH; Li, G; Radosevich, AT in [Lecomte, Morgan; Lipshultz, Jeffrey M.; Kim-Lee, Shin-Ho; Li, Gen; Radosevich, Alexander T.] MIT, Dept Chem, Cambridge, MA 02139 USA; [Kim-Lee, Shin-Ho] Univ Autonoma Madrid, Fac Ciencias, Dept Quim Organ, E-28049 Madrid, Spain published Driving Recursive Dehydration by P-III/P-V Catalysis: Annulation of Amines and Carboxylic Acids by Sequential C-N and C-C Bond Formation in 2019, Cited 69. The Name is 3-Methylbenzoic acid. Through research, I have a further understanding and discovery of 99-04-7.
A method for the annulation of amines and carboxylic acids to form pharmaceutically relevant azaheterocycles via organophosphorus P-III/P-V redox catalysis is reported. The method employs a phosphetane catalyst together with a mild bromenium oxidant and terminal hydrosilane reductant to drive successive C-N and C-C bond-forming dehydration events via the serial action of a catalytic bromophosphonium intermediate. These results demonstrate the capacity of P-III/P-V redox catalysis to enable iterative redox-neutral transformations in complement to the common reductive driving force of the P-III/P-V couple.
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Reference:
Isothiazole – Wikipedia,
,Isothiazole – ScienceDirect.com