Al Mamari, HH; Al Lawati, Y in [Al Mamari, Hamad H.; Al Lawati, Yousuf] Sultan Qaboos Univ, Coll Sci, Dept Chem, POB 36,Al Khoudh 123, Muscat, Oman published N-(2-Hydroxy-1,1-dimethylethyl)-3-methylbenzamide in 2020.0, Cited 19.0. Category: isothiazole. The Name is 3-Methylbenzoic acid. Through research, I have a further understanding and discovery of 99-04-7.
The title compound, N-(2-hydroxy-1,1-dimethylethyl)-3-methylbenzamide was synthesized by reacting 3-methylbenzoyl chloride or 3-methylbenzoic acid with 2-amino-2-methyl-1-propanol. In the present report, the synthesized target compound was fully characterized by various spectroscopic methods (H-1 NMR, C-13 NMR, IR, GC-MS), its composition confirmed by elemental analysis, and its structure determined and confirmed by X-ray analysis. The importance of this compound lies in its possession of an N,O-bidentate directing group. Such a structural motif is potentially suitable for metal-catalyzed C-H bond functionalization reactions.
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Reference:
Isothiazole – Wikipedia,
,Isothiazole – ScienceDirect.com