Application In Synthesis of 3-Methylbenzoic acid. In 2019 CHEMSUSCHEM published article about C-H ALKYLATION; N-ALKYLATION; SODIUM-BOROHYDRIDE; COOPERATIVE CATALYSIS; SECONDARY-AMINES; AROMATIC-AMINES; BRONSTED ACID; HYDROGENATION; AMINATION; MILD in [Emayavaramban, Balakumar; Chakraborty, Priyanka; Sundararaju, Basker] Indian Inst Technol Kanpur, Dept Chem, Kanpur 208016, Uttar Pradesh, India in 2019, Cited 78. The Name is 3-Methylbenzoic acid. Through research, I have a further understanding and discovery of 99-04-7.
Direct reductive alkylation of amines with carboxylic acid is carried out by using an inexpensive, air-stable cobalt/triphos catalytic system with molecular hydrogen as the reductant. This efficient synthetic method proceeds through reduction and condensation, followed by reduction of the in situ-generated imine into the amine in a green catalytic process.
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Reference:
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