An article Iodine-DMSO-Catalyzed Chemoselective Biomimetic Aromatization of Tetrahydro-beta-carbolines-3-carboxylic Acid: Mechanism Study with DFT-Calculation WOS:000490895800024 published article about TETRAHYDRO-BETA-CARBOLINES; EUDISTOMIN-U; BIOLOGICAL EVALUATION; ASSISTED SYNTHESIS; ALKALOIDS; NORHARMANE; HARMANE; DERIVATIVES; UTILITY; OXIDATIONS in [Gaikwad, Sunil, V; Devkate, Manisha; Joshi, Rekha; Shinde, Rohit G.; Nikalje, Milind D.; Lokhande, Pradeep D.] Savitribai Phule Pune Univ, Ctr Adv Studies, Dept Chem, Pune 411007, Maharashtra, India; [Nadimetla, Dinesh N.; Bhosale, Sheshanath, V] Goa Univ, Sch Chem Sci, Taleigao Plateau 403206, Goa, India; [Al Kobaisi, Mohammad] Swinburne Univ Technol, Dept Chem & Biotechnol, FSET, Hawthorn, Vic 3122, Australia; [Gaikwad, Milind, V] Dr DY Patil ACS Coll, Dept Chem, Pune 411018, Maharashtra, India in 2019.0, Cited 57.0. Recommanded Product: 93-02-7. The Name is 2,5-Dimethoxybenzaldehyde. Through research, I have a further understanding and discovery of 93-02-7
A new protocol for the chemoselective aromatization of tetrahydro-beta-carboline-3-carboxylic acids to direct biomimetic one step synthesis of beta-carboline-3-carboxylic acids 2 A-L using catalytic amount of I-2 in DMSO/H+ produces very good yield. This method was also successfully extended for the aromatization of tetrahydro-beta-carboline-3-methyl esters 5 A-G as well as one-step synthesis of Marinacarbolines-D analog, respectively. Further, the mechanism and role of iodine-DMSO in aromatization has been studied by Density Functional Theory Calculation.
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