An article Palladium-catalyzed carbonylative synthesis of acylstannanes from aryl iodides and hexamethyldistannane WOS:000575167400014 published article about ACYL; KETONES; CARBOSTANNYLATION; ACYLSTANNYLATION; ALKYNES; SILYL; TIN in [Chen, Bo; Yuan, Yang; Xu, Jian-Xing; Wu, Xiao-Feng] Univ Rostock, Leibniz Inst Katalyse eV, Albert Einstein Str 29a, D-18059 Rostock, Germany; [Franke, Robert] Evonik Ind AG, Paul Baumann Str 1, D-45772 Marl, Germany; [Franke, Robert] Ruhr Univ Bochum, Lehrstuhl Theoret Chem, Univ Str 150, D-44780 Bochum, Germany in 2020, Cited 21. Quality Control of 3-Methylbenzoic acid. The Name is 3-Methylbenzoic acid. Through research, I have a further understanding and discovery of 99-04-7
In this communication, we describe a new method for the carbonylative synthesis of acylstannanes from aryl iodides and hexamethyldistannane. With Pd(PPh3)(4) as the catalyst and toluene as the solvent at 60 degrees C under 10 bar CO for 16 h, the desired acylstannanes were obtained in good to excellent yields. In order to facilitate isolation and analysis, the obtained acylstannanes were transformed into the corresponding benzoic acids by simply stirring under air for 5 h. (C) 2020 Elsevier B.V. All rights reserved.
Quality Control of 3-Methylbenzoic acid. About 3-Methylbenzoic acid, If you have any questions, you can contact Chen, B; Yuan, Y; Xu, JX; Franke, R; Wu, XF or concate me.
Reference:
Isothiazole – Wikipedia,
,Isothiazole – ScienceDirect.com