Application In Synthesis of 3-Methylbenzoic acid. Liu, Y; Battaglioli, S; Lombardi, L; Menichetti, A; Valenti, G; Montalti, M; Bandini, M in [Liu, Yang; Battaglioli, Simone; Lombardi, Lorenzo; Menichetti, Arianna; Valenti, Giovanni; Montalti, Marco; Bandini, Marco] Univ Bologna, Alma Mater Studiorum, Dipartimento Chim Giacomo Ciamician, I-40126 Bologna, Italy; [Bandini, Marco] Consorzio CINMPIS, I-40126 Bologna, Italy published Visible-Light Photoredox Catalyzed Dehydrogenative Synthesis of Allylic Carboxylates from Styrenes in 2021, Cited 47. The Name is 3-Methylbenzoic acid. Through research, I have a further understanding and discovery of 99-04-7.
The visible-light photoredox/[Co(III)] cocatalyzed dehydrogenative functionalization of cyclic and acyclic styryl derivatives with carboxylic acids is documented. The methodology enables the chemo- and regioselective allylic functionalization of styryl compounds, leading to allylic carboxylates (32 examples) under stoichiometric acceptorless conditions. Intermolecular as well as intramolecular variants are documented in high yields (up to 82%). A mechanistic rationale is also proposed on the basis of a combined experimental and spectroscopic investigation.
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