Authors Wu, YX; Ding, HL; Zhao, M; Ni, ZH; Cao, JP in ROYAL SOC CHEMISTRY published article about FUNCTIONALIZATION; METAL; IDENTIFICATION; THIOCYANATION in [Wu, Yaxing; Ding, Hongliang; Zhao, Ming; Ni, Zhong-Hai; Cao, Jing-Pei] China Univ Min & Technol, Minist Educ, Key Lab Coal Proc & Efficient Utilizat, Xuzhou 221116, Jiangsu, Peoples R China in 2020, Cited 50. Name: 1,3-Dimethoxybenzene. The Name is 1,3-Dimethoxybenzene. Through research, I have a further understanding and discovery of 151-10-0
The electrochemical-induced C-H methylthiolation of electron-rich aromatics has been accomplished via a three component cross-coupling strategy. Potassium thiocyanate (KSCN) as both the supporting electrolyte and sulfur source and methanol as the methylation reagent are used. This protocol is versatile for various (hetero)aromatic compounds such as aniline, anisole and indole. The reaction proceeds under mild conditions without any metal catalyst, exogenous oxidant and highly toxic sulfur reagent. Importantly, such an electrochemical-induced methylthiolated reaction could be easily scaled up with good efficiency.
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Reference:
Isothiazole – Wikipedia,
,Isothiazole – ScienceDirect.com