Category: isothiazole. Recently I am researching about AMIDE BOND FORMATION; AL MIXED OXIDES; N-ARYLATION; MAGNETIC NANOPARTICLES; HYDROTALCITE; ARYL; COPPER; EFFICIENT; AMINOCARBONYLATION; FORMAMIDES, Saw an article supported by the Vinati Organics Ltd.; Godrej Consumer Products Limited (GCPL); IICT-RMIT Joint Research program; J.C. Bose grant; GCPL; J.C. Bose National Fellowship (DST, GoI). Published in ELSEVIER in AMSTERDAM ,Authors: Samudrala, PS; Nakhate, AV; Gupta, SSR; Rasal, KB; Deshmukh, GP; Gadipelly, CR; Theegala, S; Dumbre, DK; Periasamy, S; Komandur, VRC; Bhargava, SK; Mannepalli, LK. The CAS is 93-02-7. Through research, I have a further understanding and discovery of 2,5-Dimethoxybenzaldehyde
Hydrotalcite-derived (HT-derived) oxide catalysts were synthesised from hydrotalcite-like (HT-like) materials prepared by co-precipitation method (Cu-Al, Cu-Fe, Mg-Al, Mg-Fe, Ni-Fe and Ni-Al) followed by calcination and their catalytic activity was studied for oxidative amidation of carboxylic acids and substituted benzaldehydes with N,N-dimethylformamide (DMF). Catalyst screening was done using benzoic acid and DMF as a model reaction. Subsequently, we have optimised the reaction with different reaction parameters, catalyst loading, temperatures and oxidants. Cu-Fe HT-derived oxide catalyst showed excellent activity towards oxidative amidation using TBHP as an oxidant at 80 degrees C in 10 h. The fresh and spent catalysts were thoroughly characterised by different analytical techniques; XRD, SEM, HRTEM, TPD, N-2 adsorption-desorption isotherm and XPS. Moreover, the catalyst was easily separated by simple filtration and reused up to four cycles without significant loss in catalytic activity.
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Reference:
Isothiazole – Wikipedia,
,Isothiazole – ScienceDirect.com