Application In Synthesis of 1,3-Dimethoxybenzene. Cabrera-Lobera, N; Velasco, N; Sanz, R; Fernandez-Rodriguez, MA in [Cabrera-Lobera, Natalia; Velasco, Noelia; Sanz, Roberto] Univ Burgos, Fac Ciencias, Dept Quim, Area Quim Organ, Pza Misael Banuelos S-N, Burgos 09001, Spain; [Fernandez-Rodriguez, Manuel A.] Univ Alcala De Henares, Fac Farm, Dept Quim Organ & Quim Inorgon, Campus Cient Tecnol,Autovia A-2,Km 33-1, Madrid 28805, Spain published Bronsted acid-catalyzed synthesis of tetrasubstituted allenes and polysubstituted 2H-chromenes from tertiary propargylic alcohols in 2019, Cited 62. The Name is 1,3-Dimethoxybenzene. Through research, I have a further understanding and discovery of 151-10-0.
A practical and environmentally benign Bronsted acid-catalyzed protocol for the preparation of all-carbon tetrasubstituted allenes, consisting in the direct S-N’ addition of tri- or dimethoxy arenes or allyltrimethylsilane to tertiary propargylic alcohols, has been developed. In addition, a straightforward synthesis of densely substituted 2H-chromenes by metal-free tandem allenylation/heterocyclization reaction of methoxyphenols and tertiary alkynols is presented. (C) 2019 Elsevier Ltd. All rights reserved.
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