Product Details of 93-02-7. Recently I am researching about CARBON QUATERNARY STEREOCENTERS; 6+3 CYCLOADDITION; MESO COMPOUNDS; GENERATION; CONSTRUCTION; PRESSURE; SULFUR; DENDRALENES; THIOPHENES; SULFONIUM, Saw an article supported by the Austrian Science Fund FWFAustrian Science Fund (FWF) [P31023-NBL]; Center for Molecular Biosciences CMBI; Tyrolean Science Fund TWF [UNI-0404/2340]. Published in AMER CHEMICAL SOC in WASHINGTON ,Authors: Haut, FL; Habiger, C; Speck, K; Wurst, K; Mayer, P; Korber, JN; Muller, T; Magauer, T. The CAS is 93-02-7. Through research, I have a further understanding and discovery of 2,5-Dimethoxybenzaldehyde
Here we present a comprehensive study on the [3+2]-cycloaddition of thiocarbonyl ylides with a wide variety of alkenes and alkynes. The obtained dihydro- and tetrahydrothiophene products serve as exceptionally versatile intermediates providing access to thiophenes, dienes, dendralenes, and vic-quarternary carbon centers. The use of high-pressure conditions enables thermally unstable, sterically encumbered or moderately reactive substrates to undergo the cycloaddition under mild conditions, thereby increasing the yield by up to 58%. In addition, we showcase its utility by the formal syntheses of the pharmaceuticals NGB 4420 and tenilapine.
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Reference:
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