I found the field of Chemistry; Science & Technology – Other Topics very interesting. Saw the article Electrochemical anion pool synthesis of amides with concurrent benzyl ester synthesis Electronic supplementary information (ESI) available. See DOI: 10.1039/C9GC00707E published in 2019. Product Details of 93-97-0, Reprint Addresses Vannucci, AK (corresponding author), Univ South Carolina, Dept Chem & Biochem, Columbia, SC 29208 USA.. The CAS is 93-97-0. Through research, I have a further understanding and discovery of Benzoic anhydride
An electrosynthesis method for amide bond formation has been developed in an attempt to increase the atom economy for this class of reactions. This anion pool method electrochemically generates strong nucleophiles from amine substrates. The amine nucleophiles then react with acid anhydrides to generate amides, and the by- product from this reaction undergoes further chemical transformations to generate pharmaceutically relevant benzoic esters. These one- pot reactions are operationally simple, are performed at room temperature, and avoid rare transition metals and added bases. The amide synthesis is amenable to primary and secondary amines and a variety of anhydrides with yields up to 90% obtained. Atom economy and process mass index ( PMI) values calculated for this procedure indicate that this process can be considered greener compared to traditional amide synthesis routes used by industry. Furthermore, this electrochemical approach showed unique selectivity when substrates that contained two inequivalent amine moieties were examined.
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Reference:
Isothiazole – Wikipedia,
,Isothiazole – ScienceDirect.com