Recently I am researching about PHOTOREDOX CATALYSIS; ALKYLIDENECYCLOPROPANES; CYCLOADDITIONS; ALKYNYLIDENECYCLOPROPANES; TRANSMETALATION; HETEROCYCLES; ALKENES, Saw an article supported by the Strategic Priority Research Program of the Chinese Academy of SciencesChinese Academy of Sciences [XDB20000000]; National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21372250, 21121062, 21302203, 20732008, 21772037, 21772226, 21861132014, 91956115]; Shenzhen Nobel Prize Scientists Laboratory Project; [sioczz201808]. Published in ROYAL SOC CHEMISTRY in CAMBRIDGE ,Authors: Liu, JX; Wei, Y; Shi, M. The CAS is 99-04-7. Through research, I have a further understanding and discovery of 3-Methylbenzoic acid. Safety of 3-Methylbenzoic acid
We report a direct single-electron oxidation of methylenecyclopropanes (MCPs) for the rapid construction of 4-aryl-1,2-dihydronaphthalene derivatives by merging visible light photoredox catalysis and cobalt catalysis. In MeCN with Et3N center dot 3HF (1.0 equiv.), the fluorination of MCPs can be realized in the presence of 9-mesityl-10-methylacridinium perchlorate and Co(dmgH)(2)PyCl, affording fluorinated 4-aryl-1,2-dihy-dronaphthalene derivatives in moderate yields. In MeCN/HFIP (7 : 3), 4-aryl-1,2-dihydronaphthalene derivatives were obtained in good yields through a MHAT process under similar conditions.
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Reference:
Isothiazole – Wikipedia,
,Isothiazole – ScienceDirect.com