Application In Synthesis of 1,3-Dimethoxybenzene. Dusel, SJS; Konig, B in [Duesel, Simon Josef Siegfried; Koenig, Burkhard] Univ Regensburg, Inst Organ Chem, Univ Str 31, D-93053 Regensburg, Germany published Oxidative Photochlorination of Electron-Rich Arenes via in situ Bromination in 2020, Cited 41. The Name is 1,3-Dimethoxybenzene. Through research, I have a further understanding and discovery of 151-10-0.
Electron-rich arenes are oxidatively photochlorinated in the presence of catalytic amounts of bromide ions, visible light, and 4CzIPN as organic photoredox catalyst. The substrates are brominated in situ in a first photoredox-catalyzed oxidation step, followed by a photocatalyzed ipso-chlorination, yielding the target compounds in high ortho/para regioselectivity. Dioxygen serves as a green and convenient terminal oxidant. The use of aqueous hydrochloric acid as the chloride source reduces the amount of saline by-products.
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Reference:
Isothiazole – Wikipedia,
,Isothiazole – ScienceDirect.com