Application In Synthesis of 2,5-Dimethoxybenzaldehyde. Settipalli, PC; Reddy, YP; Gudise, VB; Anwar, S in [Settipalli, Poorna Chandrasekhar; Reddy, Yeruva Pavankumar; Gudise, Veera Babu; Anwar, Shaik] Vignans Fdn Sci Technol & Res, Dept Sci & Humanities, Div Chem, Guntur 522213, Andhra Pradesh, India published Knoevenagel-Friedel-Crafts-Hemiketalization Triple Cascade Reaction: A Diastereoselective Formal [1+2+3] Cyclization Towards Indenonaphthopyran Scaffolds in 2021.0, Cited 70.0. The Name is 2,5-Dimethoxybenzaldehyde. Through research, I have a further understanding and discovery of 93-02-7.
A simple and efficient cascade reaction via formal [1+2+3] cyclization of 1,3-indanedione, aldehyde and 2-naphthol is reported using K2CO3 as a base. The advantage includes metal-free conditions, varied substrate scope and shortened reaction duration with high diastereoselectivity (i. e., 99 : 1) resulting in the formation of two carbon-carbon as well as two carbon-oxygen bonds through Knoevenagel-Friedel-Crafts-Hemiketalization sequence resulting in three contiguous stereocenters.
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Reference:
Isothiazole – Wikipedia,
,Isothiazole – ScienceDirect.com