Archives for Chemistry Experiments of 27148-03-4

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Electric Literature of 27148-03-4, Chemistry is traditionally divided into organic and inorganic chemistry. The former is the study of compounds containing at least one carbon-hydrogen bonds.In a patent£¬Which mentioned a new discovery about Electric Literature of 27148-03-4

Structural study of thiosaccharin by single crystal X-ray diffraction and infrared spectroscopy

The structure of thiosaccharin (1,2-benzisothiazol-3(2H)-thione 1,1-dioxide) has been investigated by X-ray diffraction and infrared spectroscopic methods.The compound crystallizes in the orthorhombic space group Fdd2 with a = 26.591(3), b = 25.058(3), c = 4.934(5) Angstroem, Z = 16.The structure consists of thiosaccharin molecules bonded to each other through N-H<*>O intermolecular hydrogen bonds.The infrared spectra of the thiosaccharin at room and liquid-nitrogen temperature were recorded.The spectral features in the N-H stretching region were correlated with the crystallographic data on the geometry of the N-H<*>O hydrogen bonding.In an attempt to assign the bands due to the SO2 stretching modes, the spectrum of thiosaccharin was compared with that of saccharin (1,2-benzoisothiazole-3(2H)-one, 1,1-dioxide.KEY WORDS: Thiosaccharin, infrared spectra, crystal structure polymorphs.

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Reference£º
Isothiazole – Wikipedia,
Isothiazole – ScienceDirect.com